1084 HT fail

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Nov 4, 2015
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Forgive the long post, I'm trying to get as much of the story and as many of the details as I can right up front.

I'm a hobbyist and just starting out with bladesmithing. I've made a few stock removal knives from files, a few crude punches / wood chisels and a pair of rebar tongs from forging, and am now getting into making blades from scratch. For the time being, I'll be doing stock removal primarily. I've read through the stickies as well as countless other threads on several forms to collect as much info as I can process. Now I just need more hands-on practice.

I have a small 50 cal ammo can propane forge with a venturi burner that does well at getting things hot, but doesn't have much for temperature control. I'm using a 50 cal ammo can with about 1.5-2 gallons of canola oil for quenching, always heated to around 130F (+/- 10F, tested with a meat thermometer). Finally, I just picked up a small used kiln (Thermolyne 1300), and have a larger one on the way. I'm using 3/16 1084 bar stock purchased from two different reputable sellers on a major auction site.

My first several trial runs were using the forge exclusively. I heated several pieces of 1084 well past magnetic (oops) and quenched them in the warm oil, moving them back and forth from point to tang while submerged. The oil flared up quite a bit during the quench. After about 10-15 seconds, I'd remove them from the oil and allow them to finish cooling in still air. I tempered two of the pieces at 450F for an hour, cooled, and then another hour at 450F. Three other smaller test pieces were left untempered. After removing the decarb, I noticed that a file easily bit into one knife, and bit decently into the second one. I recall quenching the second knife several shades lower than the first, but still non-magnetic. Would the higher temperature (1600-1700F guestimated by shade) before quench on the first knife cause the low hardness? I shelved the first knife, and will be completing the second (harder) one to see how it ends up performing.

Ok, so a few failures at temperature control; whatever, life goes on, right? Here's where I'm stuck: the small test pieces that I didn't temper are also very tough, not brittle like I was expecting. Like the first knife mentioned above, they were most likely quenched well above the ideal temp (guestimating medium orange) and into 130F canola oil. I was able to put each one into a vise and smack them with a hand sledge until they were bent at a 90+ degree angle. Though they were more difficult to bend than similarly sized mild steel, none of them showed any cracks or other signs of stress. It's almost like they were annealed instead of hardened, despite being oil quenched very hot. I left them to sit, untempered, on my work bench for a few days, and no cracks have formed.

A few days later, my kiln showed up. I cranked it up to 1100C (~2000F) with a piece of mild steel inside as a baseline test, primarily to make sure it would reach the max temperature without blowing a fuse or tripping a breaker. Unfortunately I don't have a pyrometer, but I can say that the piece was at least a very bright orange, perhaps slightly brighter than the 1600-1700F pieces I had previously heated in the forge, perhaps dull yellow at most. The piece did start to stick to the bottom of the kiln (major pucker moment), which I didn't experience with any other samples after lowering the kiln temp. I reset the kiln for 815C / ~1500F and allowed it to cool down to the target temp, and then put two new pieces of ~2" x 2" x 3/16" 1084 in for testing. They were allowed them to soak for about 10 minutes, just to be sure, and then taken out one at a time for quench. Stupidly, I didn't test them on a magnet, but noted that both were a dull to medium red color (cloudy evening). I noticed that the oil didn't flare up with either piece, unlike the higher temp trials with the forge. Once again, without tempering, I put them into the vise and smacked them with a sledge. Both of them were able to bend at 90 degree angles with no cracks, though they took a significant amount of force to do so. I also noticed that a file skated decently well on both pieces. I was under the impression that if they were hard enough to skate a file, they should break rather than bend to that degree.

So that's where I'm at. I'm sure my temperature control needs the most work, but I was hoping to be able to break some of the sample pieces to check out the grain. So far, I haven't been able to do that. Perhaps I've been ~100-200 degrees too high in the forge, and ~100-200 degrees too low in the kiln (faulty thermocouple?). Maybe I'm taking too long getting them into the oil, or not moving them around enough during the quench. Maybe I'm taking them out of the oil too quickly. Maybe I bought questionable steel. Either way, I figured I'd have some luck by now - or perhaps I have, and I'm just expecting the untempered samples to shatter too easily.

Any suggestions?
 
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Sounds like you got crap steel...

Stay away from flea bay and buy some steel from alpha knife supply, admiral, New Jersey steel baron, or another known supplier that specializes in knife steel.

Take a couple of your scraps and heat them up to just past non-magnetic and quench them in water. Then check with a file, then try to break them. If they don’t perform at that point it’s kinda pointing to bad steel.
 
Sounds like you got crap steel...

Stay away from flea bay and buy some steel from alpha knife supply, admiral, New Jersey steel baron, or another known supplier that specializes in knife steel.

Take a couple of your scraps and heat them up to just past non-magnetic and quench them in water. Then check with a file, then try to break them. If they don’t perform at that point it’s kinda pointing to bad steel.

Gotcha, thanks. Does it matter how big the scraps are? Can I get by with something that's 1/4" x 1/4" x 3/16", or should I be using larger samples?

I do have some steel on the way from Alpha Knife Supply, though only some 80CRV2, 15N20, and 8760 to experiment with. I suppose if I can't get those to work, I'll step back down to 1084 and order it from a reputable shop this time.
 
From what I understand, 80CRV2 is even more forgiving than 1084, in terms of HT...

As far as the size goes, just lop a piece off of one of your knives... at this point it’s just a paperweight right? By sacrificing one you might be able to figure out what’s wrong...
 
Definitely buy steel from known suppliers. Hard way to learn that lesson. I'd highly recommend investing in a thermocouple and PID both can be bought cheap from ebay. It makes life ALOT easier
 
Sure enough, that's one of the sellers I bought from. The other was knifemaking_supplies. I'll have to test the samples separately to see if there's any hope for any of it. Lesson learned! Thank you.

You got ripped off, so much for "reputable sellers". The only sellers on eBay that I would buy steel from are Alabama Damascus Steel and Maker Material Supply, both of whom have their own legit websites to buy directly from. Otherwise, better to stick to the long time respected suppliers listed in the sticky threads in this forum (AKS, NJSB, Jantz, Pop's, K&G, and all them others I left out but are in the sticky).
 
Definitely buy steel from known suppliers. Hard way to learn that lesson. I'd highly recommend investing in a thermocouple and PID both can be bought cheap from ebay. It makes life ALOT easier

The furnace I used has a digital readout with the ability to set a target temperature (via analog knob that controls the digital readout). Would I be able to use a thermocouple and PID to get a "second opinion" temperature?

Thanks for the advise guys. At least it was a cheap lesson learned; less than $20 worth of steel.
 
The furnace I used has a digital readout with the ability to set a target temperature (via analog knob that controls the digital readout). Would I be able to use a thermocouple and PID to get a "second opinion" temperature?

Thanks for the advise guys. At least it was a cheap lesson learned; less than $20 worth of steel.

You might want to consider filing a complaint with Ebay once you determine who sold you the junk.
 
I use one of those "melt at this degree" markers to make sure I'm at least to the temp I'm shooting for. They're cheap and might help check your thermocouple is in the ballpark.
 
Interesting update. I cut a couple pieces from the 1084 bar stock I received from knifemaking_supplies, and another from a piece of 1095 I was given for Christmas (unknown source, likely a seller on Amazon). I'm cutting with a metal-bladed circular saw, so all of the pieces were too hot to hold when they first dropped.

The 1084 pieces were 2" x 3/4" x 3/16" and 2" x 1/2" x 3/16". 1095 was 1-3/4" x 1/4" x 3/16". I figured by keeping them small, I could better guarantee even and thorough heating.

I heated them up in the propane forge to about a medium orange and checked to ensure they were non-magnetic. I let one 1084 piece cool slowly in the air to a medium/bright red color while still ensuring non-magnetic, then dropped it into a bucket with ~10 gallons of water. The other 1084 piece and the 1095 piece were both dropped in straight from the forge, probably more in the 1600-1700F range.

This time I was able to break all three samples. The 1084 was still decently tough and took quite a few hits before breaking relatively cleanly in two. The 1095 took one quick hit and shattered into three pieces. All three unquestionably skate a file with no issue.

I'm fairly sure now that these are at least medium to high carbon steel of some form, and I'm going to test my previous 1084 samples again to make sure they weren't a fluke. I'm fairly sure that what I bought from knifemaking_supplies is legit (or at least in the ballpark), and what I bought from jimcurtjame is mild steel. Lesson learned - buy from a well-established, reputable source. ;)
 
Tonight I reheated the piece from knifemaking_supplies that I was previously able to bend at a 90 degree angle. I got it just above non-magnetic and quenched it in water. This time a sharp blow to the corner fractured it, and there are stress cracks all over the piece. So, I guess I'm ok with that batch. Now I just need to figure out why it didn't harden when quenched in oil...
 
" ….I heated them up in the propane forge to about a medium orange and checked to ensure they were non-magnetic. I let one 1084 piece cool slowly in the air to a medium/bright red color while still ensuring non-magnetic, …"

If you did the failed HT this way, I think this is where your problem was.
Proper HT is to increase the temperature to the target and not above. You should not overheat and then let drop to the target if using non-magnetic as the gauge of temperature. Non-magnetic is only useful to determine the temp in HT when observed as a rising temperature. It will be somewhere around 1414°F climbing (Ac). The non-magnetic point of change on receding temperatures (Ar) is different than on rising temps - Ar is lower than Ac.
 
" ….I heated them up in the propane forge to about a medium orange and checked to ensure they were non-magnetic. I let one 1084 piece cool slowly in the air to a medium/bright red color while still ensuring non-magnetic, …"

If you did the failed HT this way, I think this is where your problem was.
Proper HT is to increase the temperature to the target and not above. You should not overheat and then let drop to the target if using non-magnetic as the gauge of temperature. Non-magnetic is only useful to determine the temp in HT when observed as a rising temperature. It will be somewhere around 1414°F climbing (Ac). The non-magnetic point of change on receding temperatures (Ar) is different than on rising temps - Ar is lower than Ac.

Ah ha, good to know. These early trials were just using a propane forge and going by eye, so temperature control was spotty at best. Now that I have a kiln, I'll try to hit the exact temp and see how it goes.

For the blade I made previously out of real 1084, can I just normalize it and then austenize and quench again? The edge is ground fairly thin at this point, but it's still not the final edge; if it warps, I should be able to straighten it and grind some more.
 
I wouldn't bother to normalize it at this pointy. Just grind the edge back a tad and re-do the HT and see if the blade gets harder.
 
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