High temp molten salt pot for HTing stainless/HSS

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We have successfully using digital-controlled low temp salt pot for quenching and tempering carbon steel like 52100, 5160 or O1 for a while.

It is definitely a great and worth equipment since it will significantly reduce chance of distortion by large margin. By quenching the blade at slightly above MS and equalize for short time resulting a harder as quenched and noticeable tougher blade too. It properly beacuse the slower and more uniformly distribution of martenite forming and auto tempering effect.




The next project would be high temp salt for austenitizing purpose but this time I aimed for HTing stainless/high speed steel.

The reason why I want to try high-temp salt because in theory, molten salt HTing will significantly shorten the soaking time thus minimize grain growth and primary carbide agglomeration. Potentially better and finer grain that can't be achieved with vacuum or atmosphere HT environment.

But the high temp salt pot gonna be much more dangerous and challenging. I have never seen any knife makers who use salt to HTing high alloy steel before. I pretty sure Cashen, Wheeler and others ABS member who use high temp salt are only working with low alloy carbon steel.

But to operated 2200F salt may require some knowledge about material properties that why I need to ask for suggestion here. Noted that I would use digital-controlled electric kiln to do the pre-heating.

From what I planned, the heating method would be gas-fired immersion tubes. The tube gonna be salt container.
The dimension of the tube would be about 8" diameter x 24" x 0.5" wall thickness. But I'm not sure if 304 or 416 tube has heat/corrosion resistance enough to withstand the direct fire and 2000F+ molten salt in long term.

Anyone have knowledge or experience about that? Otherwise I may have to get titanium tube which will cost me over 2,000 USD just fore the tube alone.


The second part is the quench media. Low temp salt would be the ideal but my molten salt can be operated at only 650F maximum. From what I have seen most HSS/cold work data sheet require quenching in 1000F molten salt. Not sure what will happen if I quench them in 400F salt?

I would appreciate any opinion especially from the expert who working and having real experience in these filed like Larrin or Devin Thomas.
 
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There is a company in Providence, RI called Metalurgical Solutions that specialized in HT'ing HSS in salt.
 
We have successfully using digital-controlled low temp salt pot for quenching and tempering carbon steel like 52100, 5160 or O1 for a while.

It is definitely a great and worth equipment since it will significantly reduce chance of distortion by large margin. By quenching the blade at slightly above MS and equalize for short time resulting a harder as quenched and noticeable tougher blade too. It properly beacuse the slower and more uniformly distribution of martenite forming and auto tempering effect.




The next project would be high temp salt for austenitizing purpose but this time I aimed for HTing stainless/high speed steel.

The reason why I want to try high-temp salt because in theory, molten salt HTing will significantly shorten the soaking time thus minimize grain growth and primary carbide agglomeration. Potentially better and finer grain that can't be achieved with vacuum or atmosphere HT environment.

But the high temp salt pot gonna be much more dangerous and challenging. I have never seen any knife makers who use salt to HTing high alloy steel before. I pretty sure Cashen, Wheeler and others ABS member who use high temp salt are only working with low alloy carbon steel.

But to operated 2200F salt may require some knowledge about material properties that why I need to ask for suggestion here. Noted that I would use digital-controlled electric kiln to do the pre-heating.

From what I planned, the heating method would be gas-fired immersion tubes. The tube gonna be salt container.
The dimension of the tube would be about 8" diameter x 24" x 0.5" wall thickness. But I'm not sure if 304 or 416 tube has heat/corrosion resistance enough to withstand the direct fire and 2000F+ molten salt in long term.

Anyone have knowledge or experience about that? Otherwise I may have to get titanium tube which will cost me over 2,000 USD just fore the tube alone.


The second part is the quench media. Low temp salt would be the ideal but my molten salt can be operated at only 650F maximum. From what I have seen most HSS/cold work data sheet require quenching in 1000F molten salt. Not sure what will happen if I quench them in 400F salt?

I would appreciate any opinion especially from the expert who working and having real experience in these filed like Larrin or Devin Thomas.

http://www.bssa.org.uk/topics.php?article=42
http://www.azom.com/article.aspx?ArticleID=1175
 
One of my friends uses the high temp. salt pot for all his stainless work that I know of. It sure works smooth. You do need to have special high temp. salt to be able to go ahead with this.The only problems he had was when he original placed his temp. probe very deep. Yes, he built it all.
Frank
 
We have successfully using digital-controlled low temp salt pot for quenching and tempering carbon steel like 52100, 5160 or O1 for a while.

It is definitely a great and worth equipment since it will significantly reduce chance of distortion by large margin. By quenching the blade at slightly above MS and equalize for short time resulting a harder as quenched and noticeable tougher blade too. It properly beacuse the slower and more uniformly distribution of martenite forming and auto tempering effect.




The next project would be high temp salt for austenitizing purpose but this time I aimed for HTing stainless/high speed steel.

The reason why I want to try high-temp salt because in theory, molten salt HTing will significantly shorten the soaking time thus minimize grain growth and primary carbide agglomeration. Potentially better and finer grain that can't be achieved with vacuum or atmosphere HT environment.

But the high temp salt pot gonna be much more dangerous and challenging. I have never seen any knife makers who use salt to HTing high alloy steel before. I pretty sure Cashen, Wheeler and others ABS member who use high temp salt are only working with low alloy carbon steel.

But to operated 2200F salt may require some knowledge about material properties that why I need to ask for suggestion here. Noted that I would use digital-controlled electric kiln to do the pre-heating.

From what I planned, the heating method would be gas-fired immersion tubes. The tube gonna be salt container.
The dimension of the tube would be about 8" diameter x 24" x 0.5" wall thickness. But I'm not sure if 304 or 416 tube has heat/corrosion resistance enough to withstand the direct fire and 2000F+ molten salt in long term.

Anyone have knowledge or experience about that? Otherwise I may have to get titanium tube which will cost me over 2,000 USD just fore the tube alone.


The second part is the quench media. Low temp salt would be the ideal but my molten salt can be operated at only 650F maximum. From what I have seen most HSS/cold work data sheet require quenching in 1000F molten salt. Not sure what will happen if I quench them in 400F salt?

I would appreciate any opinion especially from the expert who working and having real experience in these filed like Larrin or Devin Thomas.
I know it is old thread but for one question to open other new one ? Ok , my friend i will build low temperature salt pot , i need it for some testing with 52100 and bainite ..........
Can stainless steel be quenched in this low temperature salt pot ? Did you ever try that ? If it is possible no reason for me to search for thick aluminium plates.
 
I know it is old thread but for one question to open other new one ? Ok , my friend i will build low temperature salt pot , i need it for some testing with 52100 and bainite ..........
Can stainless steel be quenched in this low temperature salt pot ? Did you ever try that ? If it is possible no reason for me to search for thick aluminium plates.

I have been quenching D2, N695, 3V, M390, Sleipnir and DC53 which are all high alloy steel in 180-190c salt with good result, the hardness we got is similar to plate/high pressure air quenching.

I also have try 52100 bainite (845c 15 min quench to 250c hold for 4 hours) at 60HRC. Bainite structure doesn't hold an edge anywhere near martensite in similar hardness tho.
 
I have been quenching D2, N695, 3V, M390, Sleipnir and DC53 which are all high alloy steel in 180-190c salt with good result, the hardness we got is similar to plate/high pressure air quenching.

I also have try 52100 bainite (845c 15 min quench to 250c hold for 4 hours) at 60HRC. Bainite structure doesn't hold an edge anywhere near martensite in similar hardness tho.
Thanks my friend :thumbsup: After quenching in salt you use plate or not ?
 
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