Darren Ellis said:
Hi Kevin, Good information here from you as usual. One question...since the temperature variations should be fairly consistent/repeatable in a given high temperature salt pot, what do you say about using a thermowell to protect the thermocouple and then doing a calibration with the standard dunk technique to find the offset?
Ok two questions... do you agitate your salts when they're up to temperature in any way? Any elegant ways to do this that you know of?
Well, let's make it three questions...as I.G. asked, I'm interested too in what type of salts you're using (for both high temp and low temp)...I know you've told us before, but I can't seem to find it...
Thanks Kevin, really appreciate you taking the time away from the shop to help answer these questions, I know I appreciate it! BTW, over on CKD (or well, the new Knife Network), there is a new heat treating forum...sure would be nice as that forum gets rolling for you to pop in from time to time there too!
-Darren
I wholeheartedly encourage testing of all sorts, as opposed to following the words of others on faith. Dunk testing while calibrating for a well may yeild good information. I have found the lag and lead times with rebound to vary on almost every heat treat job, however, so you would still be working off the assumtion that Mr. Murphy and his laws can't touch you. Either way attempting your calibration couldn't hurt, if nothing else, it would show you how much accuracy can be gained or lost with either method, and it would only be about 10 minutes of lost time.
An elegant way to agititate 1500F. salts, hmmmm, you got me on this one Darren

I give them occasional stir and let convection handle the majority. Mixing up the salts is more important with gas (due to the hot spot) than with electric. I have a couple different lengths of thermocouples and check for temp variation at differnent depths. All of my cross checking is made easier by a switch that I made out of a motor reversal drum switch. I have one lead comming out of the controller and into the switch with two leads comming out to thermocouples. One thermocouple head is labled "I" the other is "II" and the positions on the switch correspond to this. This way I can switch thermocouple readings in an instant with a flick of a lever.
Agitation is of much greater benefit in the low temp salts and I used to have a propeller driven circulator that went to the bottom of the tube and move then salts quite well. But, being the brain that I am

, I mounted the motor directly on the shaft and the heat transfred up and burned it out eventually. I have design that offsets the motor and protects it better but it would take time to make and I have been too busy to get to it, so for some time now I have benn regularly stirring my low temp as well. Of course I have the quenched piece in constant rapid motion when it goes into the salts.
As has been already discussed I use the Nusal and the Thermoquench. I am rather neurotic about having my stuff made by the guys that really know how, as opposed to me getting creative. But then I have the luxury od being able to drive to Detroit and get a 400 pound drum in 2 hours, when I need to.
Once again I encourage experimentation with the homemade mixes, but I also strongly encourage testing. One test that should be essential is to etch the blades as they come out of heat treatment (clean off the low temp first, as this stuff strongly interferes with etching). The only real damage that bad salts can do is either pit the steel (I only had this once, I don;t know what made them do it, but it was BAD), or decarburization. If your etched blade has little silver polka dots all over it, looking like somebody sprayed WD-40 near your blade right before going into the etch, then your salts are not neutral and you are losing carbon. Heatbath goes through a lot of trouble to make the salts neutral before I have to mess with them, and they also offer a graphite powder (and other specail addatives) to keep them that way.
I did not know there was heat treatment forum at the new CKD, is this new or was it there before and I didn't see it?
I am literally spending time away for the shop as I type this. This month I offically broke groudn on my addition that will be my metallurgical testing a research facility. It will be much cleaner to house all the testing equipment, microsopes and electronics. My back is killling me since I have spent the last wekk doing concrete work and laying blocks
