1095 with a partial crack in the spine--where did I go wrong?

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Jan 14, 2012
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Pardon the low quality pictures

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I figured leading in with a full shot would help other novices understand my frustration.
While the blade looks pretty, the flaw in the spine made itself apparent during my fourth etching cycle:
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The odd thing is the crack on the show side (this is for a lefty) is about a quarter inch--on the reverse side the crack is only a 24th of an inch, if that--it only appears as a slight dark spot, noticeable in the middle of this pic:
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I used those methods well noted by members such as Stacy (Bladesmith), Rick Marchand, and Tai Goo (among others) after reading Kevin's Hypereutectoid thread once a day for the past month before setting to work with Aldo's 1/8th" inch 1095. I don't typically do stock removal, but as it was my first time experimenting with 1095, I wanted to learn what I was working with before I started messing around. After reading other threads by beginners with problems with this breed, I made coupons of the steel, both beveled and non to test my HT beforehand to ensure positive results.
Satisfied, I went through the following steps:
The blank was cut from bar and profiled on my 2x72 using a dull 60grit before flat grinding to the desired levels and cleaned up using files for a steady drop to edge so that it would be neither too thin nor too thick.
I then hand sanded to 400 after drilling and deburring the handle holes. All sharp corners were softly broken starting at 200.
Once satisfied there no stress risers and the contours properly softened, I triple normalized and cleaned the blade back up to 400 grit before applying clay: the base coat was a satanite and fireclay mix, same for spine with a dab of rutland cement added-- And perhaps this is where I failed.

Both normalizing and tempering were done with a Tai inspired chunk of 2.5" muffler pipe installed in my propane forge (venturi, one of Rex's 1" hybrid burners) so that the blade did not come into contact with direct flame.
As per Stacy's standard recommendation (in threads) the blade was brought to 1,500 and allowed to soak for four minutes--I did slightly pump the blade, edge up to keep it a consistent 1, 500 while checking with a fluke laser pyrometer to make sure I did not encroach 1,550--I triple checked the Fluke's calibration using a chunk of room temp AR500 as a base to its supplied zero.
Immediately at the 4-minute mark, the blade was transferred (less than 2 seconds) to the quench--canola heated to 130 degrees (checked by candy thermometer and laser)--edge quenched 7 seconds and then completely submerged 2-3 minutes until it could be handled. I agitated during quenching by using a cutting motion so as to avoid warps or cracks.

Kitchen oven had been preheated and the blade immediately transferred from the oil to the oven for two thermal cycles at 400 degrees (again verified by thermostat in oven [not the built in one] and laser). Each thermal cycle was 2-hours, allowing the blade to cool to room temp (70 degrees) before being returned to the oven.
At the end of the second cycle, the blade was allowed to cool before I removed any remaining clay and checked with RC tester files only the 60rc just barely getting a bite.
A quick and roughed edge was free handed, and I first checked for deflection against a brass rod, then 12 penny nail, and then...yes, I know, poor form...against the rat tail on a file without chipping but finally deflecting edge just slightly, confirming I'd hit that 59-60 boundary without being too brittle.
I also know such testing is practically useless against proper Rc testing, and especially after the file test had made its own judgement, but I had to know for sure.

Satisfied with HT results, I made the slow progress up to 2K hand sanding before etching in a 4-1 ratio of PCB grade Ferric chloride warmed mildly to 60-65 degrees. I etched in 5-8 minute increments, cleaning oxides off with 2k. By the fourth cycle, I felt the sandpaper catch and, horrified, immediately neutralized.

I've now spent the past 12 hours meditating on the cause.
Too much clay? The clay was less than an eighth thick at the spine, perhaps a hair under sixteenth across the flats.
Should I have interrupted the quench? Using a 3-5 second initial edge quench, removed for a 3-count, and then completely submerged?
Among the many threads I've read on 1095 from BF, the two that stick out in my mind the most (and made a significant impression on me leading into this project) were the "Water Quench Woes" thread, and the one where one of Tai's advanced students had cracks from quenching room temp #50. Based on those threads, I wonder if, the temperature below the clay reached higher than 1,600--between pumping and trying to maintain even heat along the edge, the laser may have only read the surface of the clay, the blade below it along the spine reaching too high a temp.
The partial crack is what is most confusing--my initial edge quench might have drawn off too much heat too quickly, so that when I completely submerged, the shock caused the spine to reach its cooling point, keeping the spine straight, but still trying to warp, applying torsion, and thus the uneven break.
Or was it the spine design in and of itself? Too gentle a slope and the blade tried to curve up--causing a pileup like a car wreck.

In the meantime I've contacted the customer and informed them of the flawed blade--I consider myself fortunate that he's understanding and allowing me to make another knife. For the time being, and despite the poor picture quality, I'd appreciate some insight into where I took a misstep and ruined this blade.
 
From what you described you did everything correctly. I would recommend going ahead and breaking the blade. You can tell a lot about the crack. If the crack looks like it has oil in it or dark/black inside the cracked area then most likely it was cracked before heat treat. If it is bright and shiny then it might have happened during or after quench. The clay nor the curve issue would have caused this. You quenched in oil so the curve, if any, would have been toward the tip. But since you had a clay back it would have prevented this anyway. Do the break and examine the break. This can also tell you how your normalizing and heat went. Look for grain growth etc. I think you just had a bad piece of steel. It happens from time to time. Good luck
 
Here are my thoughts... In short form, so it may read as if I'm barking criticism but I'm not. I'm just kinda pressed for time this morning, so I can't afford a flowing paragraph before bugging out with the kids.;)

1. Not pertinent to your problem but I think you are misusing the word "tempering" in place of austenizing (or just plain heat treating). Tempering is drawing back the hardness like you did with the 400F cycles.
2. I have to ask why you felt the need to normalize Aldo's 1095 stock? ETA: I have since been told that Aldo recommends normalizing before HT. Good info for stock removers.
3. You used the muffle pipe rig and soaked your steel. How did you regulated the temperature inside the pipe? I know you had the laser but what were the heat controls.
4. You clay coated the blade and then edge quenched as well? I don't see the reasoning. You are compounding stress, IMO.
5. You left the blade in the oil and it was manageable in 2-3mins? That seems pretty quick to me. It is just as important for the blade to cool slowly as it goes past Ms as it is to rapidly cool from Ac1 down past 900F. In other words, Quench it for a 12 count (unless you are using an interupt) pull it out of the oil and set it on a brick in still air. The steel will do its thing without any help and once you can hold it with a bare hand it's ready to temper.
6. I don't know it that crack happened during the normalizations or the quench, but one of the two was the culprit. I don't think you have control of your heat yet.
7. Do you have access to a Rockwell tester? I would be curious to know the hardness in a few areas.
8. Lastly, you clearly show your lack of experience on these forums by placing me along side Stacy and Tai! Ha!:confused::eek::p

Rick
 
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Rick, after talking to Aldo last week, he recommends that all of his HC steel be normalized before HT, even when it will only be stock removal
Jason
 
Okay Jason... thanks I didn't know that. I would still normalize in bar form and not bother with trying to nail heats(in Ed's case).... just bright red, red, dull red, done. And for the final heat treat, unless you have a pyrometer in the pipe and a way of regulating heat(burner adjustments) You could be worse off trying to soak. It takes temperature and TIME for grain growth to occur and soaking affords the time.
 
Thank you gentlemen for your input--I don't mind criticism as I fully expect to be given my fair lumps in proving my place in this trade. As I said in my introductory post, I see the sheer volume of newbie makers posting and it takes time and determination for new makers to show their mettle before being accepted into the fold.

Mr. Richards--I've enjoyed looking over your work the past year and a half, having your vote of confidence makes a decidedly strong case that I was following what most tout as standard for 1095.

Rick--no offense, time is valuable to makers, when hand sanding takes as long as it does and as many orders as the primary makers who contribute to shop talk have, any words of wisdom come at a cost and I appreciate the expended time to do so.
1) Yessir, in my own haste to spit out whatever I have to say, I allow the semantics to get the better of me, a primary sin in writing (not using the jargon pertinent to the audience)--I will be sure to concrete my terminology from here out on BF and elsewhere. To not do so makes me appear less informed than I maybe.
2) I too asked Aldo and other makers if I should normalize my annealed steel prior to quenching and tempering.
3) Without PID, I've spent the past year familiarizing and tuning my venturi burner--by keeping Rex's stainless flared nozzle an inch and a quarter from the tip of the pipe and my air intake sleeve closed to the last quarter I can manage a reducing atmosphere fairly restricted at certain PSI--at 3.5-4PSI on my current setup, max temp is between 1,100-1,200. I spent several weeks last summer using the same laser thermometer tracking color shift with the laser so I could better learn color to temperature both during the day and at night. As a new maker, I know the old EyeBaller 2000 Mod 1 is no fair estimation for temperature, and did what I could to learn. For example: at 6 PSI, no muffler (direct flame impingement) and making damascus, I can easily reach welding temp in 7 minutes--by 10 the entire billet reaches even heat through and through. I'm working on a thermocouple concurrently--another tinkerer friend and I are rewriting the programming a cheap voltmeter to accept Fluke thermocouple probes. But that project, as well as others like an induction forge, are subject for another post for another day--I'm codirector of a hackerspace (read up at www.hackerspace.org) and such projects are joint inspired.

Likewise, I made a half dozen coupons of my barstock, 3 were left at their stock width, and three were given bevels similar to what I intended for the knife. All were normalized exactly the same, 1 of each (beveled and plain) were given different quenching procedures: 1 pair brought to magnetic as quickly as possible and then quenched, 1 set brought to 1,500 and allowed to soak 4 minutes, and 1 pair allowed to go to nonmagnetic and soaked ten minutes. The coupons were then cleaned up and taken to the RC tester at school--I also tested an annealed (not normalized) and a normalized piece beforehand to know where I began: annealed was 52, normalized was 54, immediately quenched were 57, the 4-min soak pair came out 59 (beveled) - 60 (nonbeveled), and the 10 minute pair came out 56. The non-soak pair had grain pattern similar to ultra fine silica sand, the 4-minute had what looked like homogeneous steel--no visible grains--and the 10 minute...well, table salt and obviously over cooked.

4) and 5) I partially submerged the initial 7 seconds along the edge line and then as I'd described above: in, 7-mississippi, complete drown--that based on the recommendation of other bladesmiths I'd asked before hand. I'm guessing as to how long she was completely submerged when I say 2-3 minutes--I was as anxious as a horse at the gate and waited just a quick 30 count as soon as the bubbling ceased before pulling. Time in all from the point she quit bubbling, pulled from oil, set in a steel tempering rack and then put in the oven had to be 8-10 minutes. That's pull, wipe excess, check against strong light (edge wise) for cracks, stick in its slot edge up, carry inside, put in oven. that is, again, quenched, quit bubbling, and then 8 minutes later in the oven.

6) Crack had to occur during quench--you and several others might call BS on this, but I felt no demarcation after normalizing along that line. There was nothing to suggest change in grain size prior to quenching the blade along the fault-line where the crack is now. I broke the blade, and there's a slight straw hue in the crack area. grain size is silky up to the crack, when it takes on a fine sparkly silica look, but still too small to see granules clearly.

7) Thanks to my role at the Valdosta State University Hackerpace, the folks in geosciences love me (I'm building their 3D printer after all) and so they allow me to play with both their RC tester and XFR analyzer. Let me know where you want tested and I'll take it over monday.

8) And I say this with my most heartfelt sincerity...skill, talent, experience, and training are all different creatures. We can look at men like Ford Hallam or A. S. Jordan and admire their work and dedication--their journey to seek perfection has led them all over the world, seeking instruction in places like Sweden, Holland, and Japan. There there's men like Jay fisher who are so exacting and disciplined in what they do that, well, Jay's catalog of designs easily spans 400 patterns, and his site is as comprehensive as they come--a loft of folks are turned off by his perceived gruffness in his writing style, but he's simply a man who knows his style and doesn't have time for froo-froo kibbitzing. Then we have guys like Tai...Tai's downtime WIP has been incredibly informative and yet, the man brings the funny. His sense of humor demonstrates his love--as precise (and sometimes unconventional) as his methods are, he is never too serious.
Be that all well and good, and this is directed directly at Rick--your technique and blending of styles represents just how much bladesmithing is a calling for you. Same as to be said about such guys as Patrice and Nick (Wheeler).
Trust me in this--I maybe a dumbsh*t newbie (and willing to admit I'm one) but I was heavily ingrained in the firearms industry, particularly signature grade 1911s. I got to chip in my two cents on some fairly big projects in that industry, and I'll avoid name dropping--the point isn't where my opinion and knowledge in firearms matches your own in blades...it's the fact I have had the pleasure of knowing folks in the custom 1911 world whose characters, personalities, and passion decidedly made an impression on their work, leading them to unique accents (such as Ned Christensen's conimede and Chuck Roger's golfball front strap checkering treatments). Take your handle wrapping technique. It's as different from Tai's as it would be to someone's like Jesus Hernandez's. That variation puts you in their league--you don't just wrap and let that be that--you have you hold your wrist a particular way, you apply the superglue a certain way; and your final cinching a specific way--all of this puts you in your own league on an equal basis for those smiths I compared you to; no sir, you are a man to be reckoned in your own league for just being your own man. I don't distribute praise indiscriminately--I'd be one of those guys at a show who brings a pair of flip-down magnifiers to get that up close look--not looking for flaws, but those smaller aspects an initial glance might miss.
 
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Have you broken the blade and examined inside the crack? This is the first thing I do if I have a question as to what caused it. There are far too many variables we are not privy to to really speculate as to the actual cause. Then sometimes the tink fairy just has to visit you that day. :-*
 
Any chance of a picture of the grain?

Also, the thing as a total newbie myself that jumps out is the user of a IR thermometer.
Emisivity changes can cause variations in the temperature sensed. Improper/inaccurate temp control is a common theme I've noted with us new makers problems.


This is a question for others who'd know better than ne. Overheating by an inaccurate reading, I can see causing grain growth, but if that occured, would it contribute to a crack in the spine exacerbated by the edge quench and clay coating?
 
If the crack was at the edge I would say it was caused by over heating or too fast a quench. The clay back slows the quench thus reducing stress in that area. Also the edge quench further slowed the quench on the spine which eguals even lower stresses than normal. Because the crack occurred on the spine rather than the edge tells me something else caused this crack. A missed stress riser would be the the most likely culprit. Even with a riser, the knife would have had to have been over heated significantly for the spine to crack and not the edge. So I still feel there was probably flaw in the steel that was not seen until after the quench and polish. I have had this happen before. The most significant one was when I was using a coil spring off a D9 cat. I forged, ground, finished it to 320 then heat treated it. I began doing the final polish and was at 800 grit before the cracks appeared. The whole blade was spider webed. It gave no indication what soever prior to that point. The material had been damaged and I did not know it. Since this crack occurred on the spine I do not feel it was the stress of the quench. But there again, stranger things have happened.
 
Yes I know that the contracting edge creates some stresses on the spine but this blade is very short so the stresses are not going to be that great. And slowing things to the extent the op did souls have made the spine very soft.
 
I don't know about the crack.... Chuck is probably right but I just reread Ed's original post and those HRC numbers on his test coupon are all over the place and not making sense. I am confident that there is a false sense of heat control happening here.
 
I broke the blade, but can't get a good pic. The edge of the crack is that dun straw color--could be from the oven. Grain structure is as follows:
Edge to top of grind is silky, the area around the fracture stays a glossy fine silica sand (finer than 2k grit) and suddenly looks coarse on the crack--partially. the opposite side doesn't show this and has a milky line.
It could be there was an existing crack or gouge in that corner of the spine I did not see, during my heat, this spot could have heated faster than the rest, starting the transition back into coarse grain when I pulled it.
 
Umm, you guys do realize Aldo's a plumber right??
:D


Gotcha. As a plumber myself I should have recognized the classic Aldo's plumber's crack symptoms...

Seriously though. Pics would help.

A possible cause of the coupons variation in HRC in addition to questioning the heat control is decarb removal. Before testing how much steel did you grind off to get below the decarb layer?

Off to shoot my 1911. :-)
 
Sorry for the cramped post earlier--been working on my GIB all afternoon.

I'd read another post earlier this month by someone who'd had difficulty pinpointing his kiln's temp and was having wildly varied results in his blades before trying the coupon tests--there decarb had been mentioned and I sanded down about a couple hundreth of a layer. When I tested the unbeveled and 4-min soaked non-beveled coupon, I went ahead and ground off a full 1/32 off.
I tried to get a friend with a proper camera by to take pics but he's tied up this weekend. I'll be working on a book scanner for our library archives monday, I'll use some privilege and use the broken pieces for test shots. ;)

When Rick tells me what areas to have Rc tested, I'll be sure to do so too.
I think the general consensus here though is over cooking, even if it was just the tip. The spots near the tip maybe the biggest indication there, Berkhouse (who gets some lovely hamons with backyard treating 1095) hit me up over FaceBook and said he's seen it when a blade's soaked too long.

Here's one thing I did not consider--my forge seems to spike during damp weather, when the humidity spikes, it just feels likes it runs hotter. Forging damascus during such times is often a gamble as normal soak times drop dramatically--as in as much as four minutes. First time I noticed it, I went about forging cable damascus (1084 stuff) the normal 8-10 minute soak was too long and by the tenth heat, had lost a significant portion of the billet. The weather the night I quenched the blade was particularly foul--just damp and a bit blustery.

Next time I believe the answer lies in less soak time--I'll either have to step up plans for a PID or thermocouple, and cut my soak time by half. I'll use a more conventional style claycoat and stick to the canola--speeding up the quench won't help, especially if I end up over cooking--and if I end up over cooking again the point is moot. Between a forge that runs hot and limited measuring, the only answer is to have more defined readings.
Otherwise? Otherwise I see if I can't make friends with one of the pottery or jewelry profs and borrow their kiln.
 
No Hamon, just the quench line visible in the first shot. Etching now would kinda be useless, and I want to get good pics of the break.
 
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