3v Oil Quenching and other questions.

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Feb 15, 2016
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I've been making O1 tool steel fixed blades for a few years, but have finally purchased the equipment needed to do a successful heat treat of stainless and other "air quenching" steels.

I've scoured forums for information, and I think I have a pretty good handle on what I'm going to do for my heat treat. But there's one thing that I would like to discuss, after listening to what the vast majority say about heat treating CPM 3v.

You see, I like to use a filing jig to make my bevels. I find that the amount of control and consistency I get from it, is wonderful. Surely, I know there are other (better) ways of doing it (which is perhaps one reason I'm making this post.), but this is what I'm comfortable with right now. But that leads to a problem - plate quenching a blade that is already beveled, sounds like it would not get a proper, even, quench, since the plates would not make direct contact to the beveled edges.

The alternative, if I want to plate quench (which, as I've gathered, is the way most people do it?), is to grind the bevels AFTER quenching. But doing so with a hand file jig, sounds like a nightmare and a half. And if I did so on a grinder, then there's the heat issue (thus requiring coolant, so I don't mess up the HT.).

But, then I read the manufacturer recommended heat treat process, and it mentions interrupted oil quench. I also have read posts by Roman Landes, stating that it is his preferred method of quenching 3v. But other than few and far between posts here and there, most people seem to discourage interrupted oil quenching. Is it just that people lack experience with it, and thus can't give any advice? Or have people actually compared the two, and found plate quenching to be superior? If so, I'd love to hear the results of your experience!

Also, what about salt baths? I'll admit that I have tossed around the idea of sticking a crucible filled with salts, in my second oven, and getting it nice and soaked at exactly 1000F, and just quenching in that. That, to me, sounds like the most controlled method, which would end in the most consistent results! Or is a molten salt quench actually not as good as oil and/or plates. Or is it simply too dangerous? I'm very curious about this, since, in theory, it seems like the best method of all, yet I can find so little information about it.

Another question I have, has to do with the preheat. Once I am done soaking it at the preheat temp (1500F in this case.), would I be better off letting it stay in the oven while it ramps up to 1950F, or putting it straight into my second oven which could be at 1950F already? My ovens are only 110V and take a while to get up to 1950F.

Lastly, if I do an oil quench, as I'm currently leaning towards - Anyone have any good advice about getting the knife out of the SS foil quickly? My current idea is to use my tongs to grab the back of the pouch, then cut off the front with kitchen shears, then pull the blade out with a second pair of pliers. Then quench in oil until the steel is black (1-3 seconds, from what I gather?). I think the harder part will be getting the frame out of its pouch, since it will be bent upward for the frame lock (I'll probably use titanium for frames, in the future, but I have AEB-L stock I want to use up!).
 
I had the same problem with taking the foil off of my 0-1 blades, I would leave the back of the knife peaking out of the tightly wrapped foil about an 1" then when pulling out of the oven with the tongs on the bare steel and grab the front of the foil with a pair of pliers and whip the foil off. The decarb wasn't to bad but that was only at 1450f.
I am under the impression that a fast ramp in temp will keep the grain growth down you would not be shocking the steel if you transferred from 1500f to 1800f-1950f.
Another solution for you might be anti scale powder which protects from decarb but only good to around 1850f I think.
 
You can leave a blade in a foil packet while oil quenching. Don't put any combustibles (e.g., paper, wood, kerosene) in the packet, though, because it will cause the packet to balloon up and then you won't get a good quench. Also, putting a coating of talcum powder on your blade will keep your foil from sticking to your blade.

Jesse
 
You can leave a blade in a foil packet while oil quenching. Don't put any combustibles (e.g., paper, wood, kerosene) in the packet, though, because it will cause the packet to balloon up and then you won't get a good quench. Also, putting a coating of talcum powder on your blade will keep your foil from sticking to your blade.

Jesse

Interesting. I know I've read that some people don't put anything in their foil, anyways, and decarb is still not an issue.

Perhaps I could press it down nice and tight, in the vise, to maximize contact with the oil. It certainly would be a lot easier than trying to fiddle with 1950F foil. I also worry about damaging the blade from pulling it out when that hot, so that also wouldn't be a problem. Thanks for the advice!
 
Molten nitrate salt is definitely the best quench media you can have.

High cooling rate at beginning, equalize at MS then air cool will give you the highest martensite percentage and lower stress/distortion.

You can do it with 400F nitrate salt too.
 
The alternative, if I want to plate quench (which, as I've gathered, is the way most people do it?), is to grind the bevels AFTER quenching. But doing so with a hand file jig, sounds like a nightmare and a half. And if I did so on a grinder, then there's the heat issue (thus requiring coolant, so I don't mess up the HT.).

You and I are in the same boat. I mill my bevels, and milling hard 3V isn't a great option.

3V benefits from a relatively rapid quench but it doesn't need to be super fast. Even though the bevels don't touch in a plate quench, if it's not a full flat grind and tapered tang there's usually enough contact in a plate quench to do the job. Remember, the heat conductivity of steel is something like 10X faster than oil, and probably 100X faster than air. So the heat flows to the cooled areas of the blade that are making good contact with the plate and the entire knife cools pretty quickly, even the areas not making contact to a plate. I'll plate quench 3V and the bevels are cool enough to touch within a minute of the quench. The key is good flat plates, no trash in the pouch or seams in the way to prevent good plate contact.

If it is full flat grind and tapered tang you might have a problem.

I've air quench, oil quenched and plate quenched 3V. Plates work very well and have the benefit of helping you keep your work straight.
 
I may consider plate quenching if I do a scandi grind. But I'd still have to oil quench the frame, since the lock would be bent upward. Unless I switch to titanium, which I'm probably going to give a try.

I went ahead and quenched my current project in oil, and it seems to have turned out well, and there was no decarb even without any combustible material inside.
 
Molten nitrate salt is definitely the best quench media you can have.

High cooling rate at beginning, equalize at MS then air cool will give you the highest martensite percentage and lower stress/distortion.

You can do it with 400F nitrate salt too.

What type of setup do you use for this?
 
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