- Joined
- Mar 12, 2013
- Messages
- 1,167
First up I just want to say thank-you to everyone on BladeForums for being so welcoming and for giving me advice and encouragement as I worked my way through my steel/blade testing!
The testing thread has gotten pretty long, so I wanted to summarize the results and the lessons I learnt so that they're a bit more pleasant to read. Hopefully they'll be of value to someone else.
Just to emphasize again, these results are probably pretty specific to my heat-treatment and my blade geometry at the very least. I think they're interesting, but I'm not in any way trying to say that they're the last word on the steels involved.
These results are mainly based around impact resistance because differentiating the blades by edge-retention is extremely difficult and time consuming. I'm also focusing on hard-use knives right now so impact resistance (and abuse resistance) is a primary concern. All the steels held an edge very well from what I could see (except 440C with a bad heat-treat).
Best:
Blade 10 - CPM3V Ver2 (60.5HRC)
Blade 2 - A2 Ver1 (59.5 HRC)
Blade 5 - CPM3V Ver1 (61.1 HRC)
Blade 8 - O1 Ver2 (59.7HRC)
Blade 7 - CPM154 Ver2 (62HRC)
Blade 1 - CPM154 Ver1 (59.6 HRC)
Blade 11 - A2 Ver2 (60.5HRC)
Blade 12 - 440C Ver2 (59.5HRC)
Blade 3 - O1 forge (55-60HRC)
Blade 4 - O1 Ver1 (60.6 HRC)
Blade 6 - 440C Ver1 (59.1 HRC)
Blade 9 - A2 Ver2 (62.5HRC)
Worst:
Overall I'm happy with the outcome. I would happily make hard-use blades from any of the top 4 steels, I'm leaning toward A2 though as it's more corrosion resistant than O1, and is easier to get in a wider variety of sizes that CPM3V. It's also less expensive and easier to heat-treat, and offers very similar performance except when it's pushed to the absolute limits. CPM154 seems like it would be a good candidate too provided that my designs are adjusted to provide some extra tip strength.
Lessons learnt about heat-treatment:
1) With adequate heat-treat it seems that all the blade steels steels tested offer great edge-retention.
2) When the heat-treat is not ideal (as with 440C Ver1 in the first test) all of the properties of the blade suffer greatly.
3) Seemingly insignificant changes in the heat-treatment process can yield huge improvements in the result. Or they can be hugely detrimental.
4) Blades need to be taken to a fine finish before H/T when using anti-scale compounds.
5) If quench speeds are changed, or cryo or sub-zero treatments are introduced, tempering temperatures will need a bunch of tweaking!
6) Harder blade steel does not necessarily equal better edge retention, even in the same steel! Each steel has a sweet spot for each application.
I know that points #1 and #2 are well known and often stated, it was just interesting for me to see first-hand the huge difference that it can make. Comparing O1 Ver1 and O1 Ver2 in the list above will highlight this. Point #6 was something I was already aware of, but again it was very interesting to see the results up close.
Lessons learnt about testing:
1) Testing steels comparatively for edge retention is HARD. Really, really, hard. Lots and lots of time can be (and was) eaten by this, and my results really weren't even very useful.
2) Testing toughness/impact resistance in an informal way is relatively easy and I think it has a lot of value.
3) Testing different heat-treats is really valuable and I'll likely keep tweaking and testing. (I'm sure most makers do too)
Lsssons learnt about assuring quality:
1) A rockwell tester really is an invaluable tool. It's a shame they don't make a small version specifically for knifemakers.
2) Decarburization seems to show up as lighter colored patches after etching a blade with Ferric Chloride for a few seconds.
Some snappy fun facts about what went into the testing:
If you've gotten this far and you're still not sure what I'm talking about, check out the original thread here: http://www.bladeforums.com/forums/showthread.php/1104795-Steel-testing-underway
If anyone has critiques or suggestions for heat-treatments or test methods I'd love to hear them!
Thanks for reading along, I've very much enjoyed getting to share the process with you all!
-Aaron
---------
Here's a summary of all the heat-treatments I used in the testing:
Round 1:
CPM3V Ver1 (blade #5):
Preheat to 1500ºF, Equalize
Ramp to 2050ºF, hold for 20 minutes
Quench in air to below 125ºF
Temper at 1000ºF, 3 times, 2 hours each -> 61.1HRC
440C Ver1 (blade #6):
Preheat to 1425ºF, equalize
Ramp to 1900ºF, hold for 20 minutes
Quench in air to room temperature
Temper at 300ºF, 2 times, 2 hours each -> 59.1HRC
CPM154 Ver1 (blade #1):
Preheat to 1400ºF, equalize
Ramp to 1900ºF, hold for 60 minutes
Quench in oil to below 125ºF
Cryo-quench into dry-ice & isopropanol for 20 minutes
Temper at 400ºF, 2 times, 2 hours each -> 59.6HRC
O1 Ver1 (blade #4):
Preheat to 1250ºF, equalize
Ramp to 1500ºF, hold for 15 minutes
Quench in oil to 150ºF
Temper at 400ºF, 2 hours
Cryo-quench into dry-ice & isopropanol for 20 minutes
Temper at 400ºF, 2 hours -> 60.6HRC
A2 Ver1 (blade #2):
Preheat to 1100ºF, equalize
Ramp to 1775ºF, hold for 35 minutes
Quench in air to below 150ºF
Temper at 400ºF, 2 hours
Cryo-quench into dry-ice & isopropanol for 20 minutes
Temper at 400ºF, 2 hours -> 59.5HRC
O1 Forge (blade #3):
Heat in forge until dull cherry-red color
Quench in oil immediately
Temper at 400ºF, 2 hours, twice -> 55-60HRC
Round 2:
A2 Ver2 (blade #9 & #11):
Double coat in anti-scale (ATP-641)
Stress relieve: Ramp to 1200ºF, hold 2 hours, furnace cool to 900ºF, cool in still air to room temperature
Ramp to 1740ºF @ 400ºF/hr, hold 20 minutes
Oil quench until no longer glowing, then cool in still air to room temperature
Sub-zero treatment in dry ice and isopropanol for 45 minutes
1 blade: Temper @ 4250ºF, twice, 2hrs each time -> 62.5HRC
1 blade: Temper @ 600ºF, twice, 2hrs each time -> 60.5HRC
CPM154 Ver2 (blade #7):
Wrap in stainless foil envelope
Stress relieve: Ramp to 1200ºF, hold 2 hours, furnace cool to 900ºF, cool in still air to room temperature
Preheat to 1400ºF, hold 10 minutes
Ramp to 1900ºF, hold 60 minutes
Plate quench to ambient
Sub-zero treatment in dry ice and isopropanol for 45 minutes
Temper @ 400ºF, twice, 2hrs each time -> 62HRC
O1 Ver2 (blade #8 ):
Double coat in anti-scale (ATP-641)
Stress relieve: Ramp to 1200ºF, hold 2 hours, furnace cool to 900ºF, cool in still air to room temperature
Preheat to 1200ºF, hold 10 minutes
Ramp to 1470ºF, hold 30 minutes
Quench into oil to ambient
Sub-zero treatment in dry ice and isopropanol for 45 minutes
Temper @ 400ºF, twice, 2hrs each time -> 59.7HRC
CPM3V Ver2 (blade #10):
Enclose in stainless foil envelope
Stress relieve: Ramp to 1200ºF, hold 2 hours, furnace cool to 900ºF, cool in still air to room temperature
Preheat to 1500ºF, hold 10 minutes
Ramp to 1975ºF, hold 30 minutes
Plate quench to ambient
Sub-zero treatment in dry ice and isopropanol for 45 minutes
Temper @ 975ºF, three times, 2 hrs each time -> 60.5HRC
440C Ver2 (blade #12):
Enclose in stainless foil envelope
Stress relieve: Ramp to 1200ºF, hold 2 hours, furnace cool to 900ºF, cool in still air to room temperature
Preheat to 1500ºF, hold 10 minutes
Ramp to 1875ºF, hold 30 minutes
Plate quench to ambient
Sub-zero treatment in dry ice and isopropanol for 45 minutes
Temper @ 400ºF, 2 times, 2 hrs each time -> 59.5HRC
The testing thread has gotten pretty long, so I wanted to summarize the results and the lessons I learnt so that they're a bit more pleasant to read. Hopefully they'll be of value to someone else.
Just to emphasize again, these results are probably pretty specific to my heat-treatment and my blade geometry at the very least. I think they're interesting, but I'm not in any way trying to say that they're the last word on the steels involved.
These results are mainly based around impact resistance because differentiating the blades by edge-retention is extremely difficult and time consuming. I'm also focusing on hard-use knives right now so impact resistance (and abuse resistance) is a primary concern. All the steels held an edge very well from what I could see (except 440C with a bad heat-treat).
Best:
Blade 10 - CPM3V Ver2 (60.5HRC)
Blade 2 - A2 Ver1 (59.5 HRC)
Blade 5 - CPM3V Ver1 (61.1 HRC)
Blade 8 - O1 Ver2 (59.7HRC)
Blade 7 - CPM154 Ver2 (62HRC)
Blade 1 - CPM154 Ver1 (59.6 HRC)
Blade 11 - A2 Ver2 (60.5HRC)
Blade 12 - 440C Ver2 (59.5HRC)
Blade 3 - O1 forge (55-60HRC)
Blade 4 - O1 Ver1 (60.6 HRC)
Blade 6 - 440C Ver1 (59.1 HRC)
Blade 9 - A2 Ver2 (62.5HRC)
Worst:
Overall I'm happy with the outcome. I would happily make hard-use blades from any of the top 4 steels, I'm leaning toward A2 though as it's more corrosion resistant than O1, and is easier to get in a wider variety of sizes that CPM3V. It's also less expensive and easier to heat-treat, and offers very similar performance except when it's pushed to the absolute limits. CPM154 seems like it would be a good candidate too provided that my designs are adjusted to provide some extra tip strength.
Lessons learnt about heat-treatment:
1) With adequate heat-treat it seems that all the blade steels steels tested offer great edge-retention.
2) When the heat-treat is not ideal (as with 440C Ver1 in the first test) all of the properties of the blade suffer greatly.
3) Seemingly insignificant changes in the heat-treatment process can yield huge improvements in the result. Or they can be hugely detrimental.
4) Blades need to be taken to a fine finish before H/T when using anti-scale compounds.
5) If quench speeds are changed, or cryo or sub-zero treatments are introduced, tempering temperatures will need a bunch of tweaking!
6) Harder blade steel does not necessarily equal better edge retention, even in the same steel! Each steel has a sweet spot for each application.
I know that points #1 and #2 are well known and often stated, it was just interesting for me to see first-hand the huge difference that it can make. Comparing O1 Ver1 and O1 Ver2 in the list above will highlight this. Point #6 was something I was already aware of, but again it was very interesting to see the results up close.
Lessons learnt about testing:
1) Testing steels comparatively for edge retention is HARD. Really, really, hard. Lots and lots of time can be (and was) eaten by this, and my results really weren't even very useful.
2) Testing toughness/impact resistance in an informal way is relatively easy and I think it has a lot of value.
3) Testing different heat-treats is really valuable and I'll likely keep tweaking and testing. (I'm sure most makers do too)
Lsssons learnt about assuring quality:
1) A rockwell tester really is an invaluable tool. It's a shame they don't make a small version specifically for knifemakers.
2) Decarburization seems to show up as lighter colored patches after etching a blade with Ferric Chloride for a few seconds.
Some snappy fun facts about what went into the testing:
- 5 grinder belts of various grits
- 9 feet of various tool steels
- The kiln was on for approximately 70 hours doing heat-treatments
- 84Gb of digital video footage was taken during the testing (2 hours or so of footage)
- More than 120 sharpening sessions
- Over 150 feet of 1/4" sisal rope
- Over 36,160" linear inches of cardboard cut (3,013 feet, or just one kilometer!)
- The testing in total took more than 178 hours over 5 weeks.
If you've gotten this far and you're still not sure what I'm talking about, check out the original thread here: http://www.bladeforums.com/forums/showthread.php/1104795-Steel-testing-underway
If anyone has critiques or suggestions for heat-treatments or test methods I'd love to hear them!
Thanks for reading along, I've very much enjoyed getting to share the process with you all!
-Aaron
---------
Here's a summary of all the heat-treatments I used in the testing:
Round 1:
CPM3V Ver1 (blade #5):
Preheat to 1500ºF, Equalize
Ramp to 2050ºF, hold for 20 minutes
Quench in air to below 125ºF
Temper at 1000ºF, 3 times, 2 hours each -> 61.1HRC
440C Ver1 (blade #6):
Preheat to 1425ºF, equalize
Ramp to 1900ºF, hold for 20 minutes
Quench in air to room temperature
Temper at 300ºF, 2 times, 2 hours each -> 59.1HRC
CPM154 Ver1 (blade #1):
Preheat to 1400ºF, equalize
Ramp to 1900ºF, hold for 60 minutes
Quench in oil to below 125ºF
Cryo-quench into dry-ice & isopropanol for 20 minutes
Temper at 400ºF, 2 times, 2 hours each -> 59.6HRC
O1 Ver1 (blade #4):
Preheat to 1250ºF, equalize
Ramp to 1500ºF, hold for 15 minutes
Quench in oil to 150ºF
Temper at 400ºF, 2 hours
Cryo-quench into dry-ice & isopropanol for 20 minutes
Temper at 400ºF, 2 hours -> 60.6HRC
A2 Ver1 (blade #2):
Preheat to 1100ºF, equalize
Ramp to 1775ºF, hold for 35 minutes
Quench in air to below 150ºF
Temper at 400ºF, 2 hours
Cryo-quench into dry-ice & isopropanol for 20 minutes
Temper at 400ºF, 2 hours -> 59.5HRC
O1 Forge (blade #3):
Heat in forge until dull cherry-red color
Quench in oil immediately
Temper at 400ºF, 2 hours, twice -> 55-60HRC
Round 2:
A2 Ver2 (blade #9 & #11):
Double coat in anti-scale (ATP-641)
Stress relieve: Ramp to 1200ºF, hold 2 hours, furnace cool to 900ºF, cool in still air to room temperature
Ramp to 1740ºF @ 400ºF/hr, hold 20 minutes
Oil quench until no longer glowing, then cool in still air to room temperature
Sub-zero treatment in dry ice and isopropanol for 45 minutes
1 blade: Temper @ 4250ºF, twice, 2hrs each time -> 62.5HRC
1 blade: Temper @ 600ºF, twice, 2hrs each time -> 60.5HRC
CPM154 Ver2 (blade #7):
Wrap in stainless foil envelope
Stress relieve: Ramp to 1200ºF, hold 2 hours, furnace cool to 900ºF, cool in still air to room temperature
Preheat to 1400ºF, hold 10 minutes
Ramp to 1900ºF, hold 60 minutes
Plate quench to ambient
Sub-zero treatment in dry ice and isopropanol for 45 minutes
Temper @ 400ºF, twice, 2hrs each time -> 62HRC
O1 Ver2 (blade #8 ):
Double coat in anti-scale (ATP-641)
Stress relieve: Ramp to 1200ºF, hold 2 hours, furnace cool to 900ºF, cool in still air to room temperature
Preheat to 1200ºF, hold 10 minutes
Ramp to 1470ºF, hold 30 minutes
Quench into oil to ambient
Sub-zero treatment in dry ice and isopropanol for 45 minutes
Temper @ 400ºF, twice, 2hrs each time -> 59.7HRC
CPM3V Ver2 (blade #10):
Enclose in stainless foil envelope
Stress relieve: Ramp to 1200ºF, hold 2 hours, furnace cool to 900ºF, cool in still air to room temperature
Preheat to 1500ºF, hold 10 minutes
Ramp to 1975ºF, hold 30 minutes
Plate quench to ambient
Sub-zero treatment in dry ice and isopropanol for 45 minutes
Temper @ 975ºF, three times, 2 hrs each time -> 60.5HRC
440C Ver2 (blade #12):
Enclose in stainless foil envelope
Stress relieve: Ramp to 1200ºF, hold 2 hours, furnace cool to 900ºF, cool in still air to room temperature
Preheat to 1500ºF, hold 10 minutes
Ramp to 1875ºF, hold 30 minutes
Plate quench to ambient
Sub-zero treatment in dry ice and isopropanol for 45 minutes
Temper @ 400ºF, 2 times, 2 hrs each time -> 59.5HRC