Heat treating questions

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Aug 24, 2009
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there has been quit a bit on heat treating lately, and for me it has raised many more questions than it has answered. ive got some general questions concerning any generic knife steel, and some specific questions about CPM M4, that I cant find adequate answers because it is so different (austenitizing temp over 2100 F), additionally I cant heat treat the M4 so I have a couple of questions about professional ht.:confused:
O.k. General
1. differential quenching-Why does w2 almost allays have a sweet hamon, and also if one does differentially quench (I am assuming edge dunking, but I suppose for clay also) does the part you dunked obtain the same hardness as if you dunked the whole thing? I think since the top is not cooling through water, or oil it will transfer most of its heat to the submersed part. also if edge dunking if you normally used oil should you use water?, or if you would normally use water use a brine? or would the distortion be especially dangerous in a differential? also should the temper be at a lowere temp.? I've heard that some tools will quench (differentially), and the excess heat in the rest of the tool will temper the blade.
2. should one use a higher austenizing temp, and then temper at higher temp or austenitize lower and temper lower for the same hardness?
3. does vacuum ht reduce/eliminate decarburization? and increase consistancy

CPM M4 and prof. Ht :confused:
1 if sending out to a professional can I request a quenching medium, and will they quench differentially, or at least not quench the tang? (This one I find to be much more important than differential b/c a brittle hiden tang is bad, as well as for a skinny necker with no scales drobing it on the handle might fracture it.)
2. additionally Id like the M4 on small blads up to 64/65 will most H.t.ers do this high? Recommendations?
and if you have a heat treating kiln would you ht M4 up to 65?

Thanks in advance

[edit]
everyone using HSS must read this http://met-sol.com/pdfs/pdf0008.PDF
pay special atention to the photomicrographs, now imagine what a particle metallurgy steel would look like
salt baths are the way to go
 
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The key to achieving a hamon line is a steel that has to be quenched quickly to form martensite (the hard stuff). W2 is going to need to go from something like 1500 to under 900 in about one second, otherwise it will form pearlite (crappy, kinda hard stuff that will skate a file, but not hold an edge). M4 and other deep hardening steels (D2 for example) need to go from austenitizing temp to "under the nose" in a few minutes, not a few seconds. Thus they'll form martensite throughout the entire blade and form no quench line.

A hamon serves very little propose in most blades.

If you send M4 out and request HRC 64/65 they'll be happy to give it to you because that is a fairly typical hardness for that steel. However, for best results they recommend a salt quench, but most folks will give you a gas quench.

Even if they don't quench the tang, M4 will still get full hard. But I wouldn't worry about it being brittle, in fact it will be nearly indestructible.
 
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Thanks for your reply by the way I accidentally read The Metolography of Iron and Steel over the summer and have a very good basic (if arcaic) knowledge of structure, and heat treatment, but if there is some significant development in the past century that i havnt heard of pleas educate me. :D

edit: yeah your totaly right about the tang seeing as M4 will harden in air. I knew that :o
 
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I just got all the parts needed to build a 16A heat treat oven with programmable temperature control. Total cost was cheaper than a bar of CPM M4 haha.

I would use 2200F for full hardness. Haven't tried it yet though.
 
3 feet x 1.5 inches $126 I bet your fancy thermometer cost more than that :D

Hehe I got a ceramic-enclosed Type K thermometer for $8 shipped. They are pretty cheap and usable up to 2300F. The PID temperature controller is homemade so it was free. I paid $80 for all those firebricks though, that's what killed me. Had to sell a knife to fund that.
 
ah screw you Cotdt, did you basically follow the kiln instructions posted a day or so ago or what:D ?
have fun :D:D:D:D
 
ah screw you Cotdt, did you basically follow the kiln instructions posted a day or so ago or what:D ?
have fun :D:D:D:D

Thanks, I'll have a lot of fun with this! I've been talking to flemingknives here to help me plan my build for weeks now, since he's gone through the whole process. Good thing electric kilns are very simple devices, just a heating element in an insulated enclosure. The hard part is finding the parts locally to avoid shipping costs.

The ovens can be made a lot smaller and lighter than I expected, which is good because I move around a lot. You pretty much want to build your own because the commercial units are slow to heat up and a bit pricey. It's best to design your own oven to the maximum amount of power your house's power line can deliver.

Salt pots are better but much more expensive to build, and high temperature salts are very expensive. The people who have built them say they have a tendency to leak after a while, which will burn down house.
 
I dont differentially heat treat so I cant help you there.

As for professional heat treating thats what I currently use. They typically will have a variety of processes in house such as vacuum, salt etcetc. They have different quenching mediums and a bunch of other variables you can play with. Theres no way I would trade this level of precision for heat treating by eye IMHO theres no way it can be done reliably every time. Plus I dont want to deal with decarbusation hassles and I like to heat treat almost complete blades rather than having the hassle of finishing hardened tool steels. Plus many people overheat their blades in post heat treat finishing and wreck the heat treat in the process. You have to either use cooled polishing machines or do it by hand.
 
my thoughts exactly nullak if I'm gonna pay a lot for the M4 then I'm having it sent out b/c it seemes particularly tough to heat treat. as for the others, anything that austenizes under 2000 F I'l probly do myself
 
Anyone ever try molten lead instead of salt bath?

It would work for a low temperature temper, but would vaporize in a quench. And be toxic. And not wash off.
 
It would work for a low temperature temper, but would vaporize in a quench. And be toxic. And not wash off.

Well lead melts at 620F and boils at 3200F, I don't see why it wouldn't work. You're definitely right it's toxic and doesn't wash off easily, but the grinding should remove it.
 
Well lead melts at 620F and boils at 3200F, I don't see why it wouldn't work. You're definitely right it's toxic and doesn't wash off easily, but the grinding should remove it.


I'll be damned... :foot:

I recall from my bullet casting days that A: it melted at a fairly low temperature and B: if you got it too hot it made dangerous fumes. But yeah, I just looked it up and your data is (mostly) correct. I think it boils at 2200.

You are right, with some precautions, I don't see why that wouldn't work.
 
Maybe so, but I can think if a lot of other things I'd rather have in my shop than freaking molten lead. And grinding it off would be toxic as well and the toxic lead dust would cover everything in your shop. I personally like my health too much.

Nathan
 
Maybe so, but I can think if a lot of other things I'd rather have in my shop than freaking molten lead. And grinding it off would be toxic as well and the toxic lead dust would cover everything in your shop. I personally like my health too much.

Nathan

Good point, let's just forget the idea of molten lead. :o
 
The idea of molten lead brings images of horror movies and melting faces to my mind for some reason. :D That and impotence or babies with birth defects.

Which, upon retrospect, is no laughing matter at all :(.

--nathan
 
Molten lead HT is discussed in Tool Steel Simplified. As I recall it's a somewhat obsolete industry practice and required a protective layer on top of the lead, I vaguely remember that powered graphite is normally used for the layer.

Kevin recommended this book some time ago. Cheap used copies of several different editions are readily available. I learned a lot from it.
 
lead oxide, a red powdery substance is extremely hazardous. Any lead grinding dust left behind would oxidize, leaving this even more toxic material in its place. The reason it is so much more dangerous is that the powder clings to clothing and gets spread to car, house, furniture etc.
 
salt is used becaues it has a high heat capacity, and is very conductive, its also safe :D
 
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