Triple Quench 0-1?

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There have been a lot of questions about o-1 lately so I dug this 'out of the grave'. This is an old thread but there is a LOT of great info here!Thank you again,Kevin,this thread realy improved my understanding of what's going on.I hope it helps some of you and saves some typing time for others. Enjoy the info!!

Has anybody done any triple quench testing on 0-1? I do my heat treating w/ a torch and magnet and turn out a respectable 0-1 blade this way,[differential hardening] but would this be a suitable replacement for the soak time? My 0-1 blades seem to hold a very good edge without being brittle.Can I make them better with a proper soak?
 
I am coming to the conclusion that no method of heating does all jobs well. Electric ovens do the soak, but are less good (even lousy?) for thermal cycling to reduce the grain. Gas forge is good for forging and cycling, but harder (lots harder) to get accurate soak temperatures with. Salts do both cycling and soaking, but are a lot more complicated to set up and operate.

I am playing with O-1 and a gas forge with a hand held thermocouple read out. Not perfect, but it does help to approximate a soak.
 
. . .snip. . .Electric ovens do the soak, but are less good (even lousy?) for thermal cycling to reduce the grain. . .snip

I am afraid I am not following your logic here? I use an electric furnace for all of my O1 and have no trouble whatsoever with grain refinement.
 
I am coming to the conclusion that no method of heating does all jobs well. Electric ovens do the soak, but are less good (even lousy?) for thermal cycling to reduce the grain. Gas forge is good for forging and cycling, but harder (lots harder) to get accurate soak temperatures with. Salts do both cycling and soaking, but are a lot more complicated to set up and operate.

I am playing with O-1 and a gas forge with a hand held thermocouple read out. Not perfect, but it does help to approximate a soak.

I'm interested to know why you think ovens are bad for cycling? I think mine does an excellent job. Anytime you can control the temps well, it's a good thing. I used to use my forge for cycling (grain refinement) but I was always doing it at too low a temp, so most of my blades had alloy banding. I've switched to the oven; problem solved.
 
Normally when one finds strong positions on topics such as this I may be in the center of it, but I am going to take a more moderate position on this one. It seems no matter what one says in this business, it will be misinterpreted to some degree or distilled down to black or white.

C_Claycomb, I can see where you are coming from since it would appear the every method has at least one Achilles heal.
I would say that any method of heating can do the job for you, after all the steel doesn't know what provides the heat, just some methods have drawbacks and rely more and more upon the faulty human factor.

As I have repeated so many times in the past, it is really just a matter of matching your steel to your equipment. The more basic your equipment the more basic your steel needs to be. One can work under a shade tree on a 1955 Chevy, but one needs much more sophisticated equipment to work on a top of the line 2007 designed for racing.

The fewer tools you have the less alloying you want in the steel. The old blacksmith banged out tools and hardened in nothing but a forge and a slack tub, but his steel was nothing much more than iron and carbon. If we want to work with those tools today we need to find alloys that are still around that could be suited for it. If all one has is a torch, which is even more limited than a coal forge in heating area and atmosphere control, then one will get better results with simpler steels. The simplest we have today are the 10XX series, and of these 1080 or 1084 will yield the best results with the least amount of effort. If you get a 1084 blade up to nonmagnetic with a torch and then quench it, you may actually get enough carbon into solution to be very happy with it. If you move up to something a bit more complex like 5160 and ignoring the smidge of proeutectoid ferrite, you now have a chemistry that needs to be dealt with since chromium carbides are not simple cementite (iron carbide). Just heating it to nonmagnetic and quenching it will yield less than optimum results because you will not pull into play the needed carbon locked up in those chemical bonds with the chromium, that will require time at temperature. One way that smiths have found around this with simpler tools is to get some into solution and then quench, locking it in solution, and then reheat it to pull the next portion into solution.

Now things get more complicated (like they weren't already:rolleyes: ). If one hangs around below the magnetic point for too long that carbon will come right back out of solution and segregate. This is where a torch could work for you, with a flame that can be as hot as 6000F. it is capable of heating very localized spots incredibly fast, so smaller blades can be brought beyond nonmagnetic quickly enough to get at more carbon without losing the last bit. However without any soaking one will need to go to a much higher temperature to break those richer carbides, so if you are not really on the ball there is a good chance of growing grain and other nasties.

Torches are terrible for oxidizing and decarb, but this is off set by the quick heating and short time at temperature. Kilns are really terrible at oxidizing and decarb but are really great for holding times at temperature so all one has to do is defeat the atmosphere problems and they are there.

One can cycle in a forge, kiln or any heat source for that matter but the most critical factor is evenness of heat, for proper normalizing the heat needs to be even throughout, torches don't this very well at all, kilns can do it but slowly, this is why I prefer a forge for normalizing.

Deweyknives, 52100 is a more complex steel and will offer about a hair less of a challenge than O1 in getting proper solutions. Of course one could go the opposite direction and shoot for segregation as this is very popular among many knifemakers today and seems to be attractive to some collectors; it will cut rope like crazy as that edge quickly gets ragged and starts tearing things out of its way, something that is also very marketable today.

I am going to say it again as I figure through repetition it may begin to stick eventually- O1 is not the best steel for beginners with little equipment. Just because you can quench it in almost anything and skate a file, does not mean that you have tapped the steels true potential in any significant way. Lets look at the extra alloying in this steel- chromium, tungsten, vanadium, all in large enough amounts to hog up a lot of carbon, that is why they need to put at least .9% in there. If one wants to bring even a decent portion of it into play they will need to hold the steel at a proper temperature long enough to do it.

Many, and I mean many, folks would beg to disagree with me on this, maintaining that their 30 second soak on O1 produce blades that cut very well. I produced those same blades for some time. It was not until I started really looking at what was happening inside that O1 that I realized its true potential, and that I was only tapping a portion of it. One can get results that can rival any simpler steel by heat treating O1 without a soak, but why not just use a simpler steel that is much less expensive and get the same results with less cost and headache. If one then goes on to spend the money on more equipment they will find that O1 is capable of not just rivaling simpler steels but blowing them out of the water when cutting.
 
... I used to use my forge for cycling (grain refinement) but I was always doing it at too low a temp, so most of my blades were had alloy banding. I've switched to the oven; problem solved.

Isn't it interesting that what some go to great lengths to put into their blades, others go out of thier way to get rid of;) . It really does go to show how completely subjective performance and design is in knives:). Two guys can build knives that cannot be more opposite, and there is a market for both... DANG! I LOVE AMERICA!
 
Isn't it interesting that what some go to great lengths to put into their blades, others go out of thier way to get rid of;) . It really does go to show how completely subjective performance and design is in knives:). Two guys can build knives that cannot be more opposite, and there is a market for both... DANG! I LOVE AMERICA!

Well said. I was thinking almost the same thing while I was writing my first post. :D
 
Kevin; Thanks for the information.My intention isn't to create arguement but to gain knowledge on making a better knife. I use a torch only for heat treating as that's the way I get best control for a differential harden. For my forging,I have a charcoal forge I made to fit inside my woodstove. 14" long x 10" wide in a v shape with bottom air feed.It's safe as it's contained inside the stove,doesn't use a lot of fuel and will blister a piece of steel in short order.So heat isn't a problem,heat control IS an issue.There are no makers in my area so anything I know has come by read,do,test.I do a lot of cutting and compare to some good factory knives.As I outcut them without a problem,I can only compare the next one I make with the last.So,I ask, can I make these better? If so, how? With your information, the answer is YES!! How? Change my techniques!! That's what I'm looking for. Thank you. That's why I came here,to gain knowledge and make better knives! Thanks to all who share!
 
Great thread. Ive always wondered myself....sometimes people will swear that their multiple quenches produce odd hamons. The reply is always that you wipe the slate clean when you bring it back up to temp....im wondering now if those odd hamons arent simply an effect of multiple quenches where soak was not properly achieved.
 
Phillip; I have read the follow-up thread and just re-read. It brings me back to the original question. If you don't have very good heat control for the soak time, is there an alternative to get the best from 0-1? Will multiple quenches work? Kevin says no and I'm in no position to argue.I can't micro-analize my steel so the next question is: Get more equipment?
Use different steel?
Go way out on a limb and try to prove Kevin wrong. As kevin states,reinventing the wheel isn't very productive so I have two sensable choices. As I learn,I seek a better outcome.Isn't that what it's all about?
 
Exellent thoughts,David.As I do multiple quenches on 5160 I try to go mid-way on the blade first,a little less 2nd and a little less 3rd. I figured this would gradualy refine structure down to the cutting edge providing I don't overheat on following heats. Any thoughts?
 
Phillip; I have read the follow-up thread and just re-read. It brings me back to the original question. If you don't have very good heat control for the soak time, is there an alternative to get the best from 0-1? Will multiple quenches work? Kevin says no and I'm in no position to argue.I can't micro-analize my steel so the next question is: Get more equipment?
Use different steel?
Go way out on a limb and try to prove Kevin wrong. As kevin states,reinventing the wheel isn't very productive so I have two sensable choices. As I learn,I seek a better outcome.Isn't that what it's all about?

I guess I'd suggest using a different steel. To get the most out of O1, I really think it needs to be soaked. But you could probably easily get the most out of 1080, or 1084 using a forge for heat treating. Get some of the 1084 from Aldo in the "knifemaking supplies for sale" section. It's got enough carbon to compete with 1095 for edge holding, but it has enough manganese to make it easier to heat treat.
But if you want, go ahead and try multiple quenching O1.
It's not illegal. :D If your happy with the results, then go with it.
 
Deweyknives, it looks to me like you are well on your way to making some very fine knives, I gather this from your attitude in what you have written here. My only concern is how much faith you are willing to put into "Kevin says”. If there is one thing that I have repeated more than almost anything else in my postings on the internet, it is to not to take my word for it, but let my words cause you to question everything and spur on your own research. Blindly following any bizarre recommendations of high profile figures in a hasty pursuit of superior results, has led to what I see as many of the problems in knifemaking today. Accepting my conclusions without insisting on supporting data and facts only makes me another part of the problem.

You do not need fancy testing equipment to do your own very good research and study in quality control or R&D. What my fancy equipment has allowed me to do is more accurately interpret the results of testing. Most of what I have seen is out there is not intentional deception but hasty interpretation of results heavily influenced by the natural desire to have ones views and techniques validated.

Outperforming the better production knives is a very good standard to work with (it is after all what handmade knives are all about). You are already a step ahead of many in that you are using a more reliable control than your own previous knives, which if you are not steadily improving on, perhaps you should find another line of work. But when using those factory blades for a control be certain that you are comparing the same properties. Most of the factory blades I have worked with had an excellent heat treat that was handicapped by a poor edge geometry. This is not entirely the fault of the manufacturer since they need to make the edge to be able to take on the abuse that will be heaped upon it by careless consumers. A friend of mine in Germany named Roman Landes (I hope our conversations makes me the friend I consider him), has written a fantastic book, unfortunately not in English, that devotes a whole section to how much potential is lost in almost all knives because we need to compensate for consumer misuse.

Test your knives but at the same time continually develop an understanding of the underlying causes and effects. Don’t allow yourself to get confused by the current hyped up trends and attempts to redefine what knives are for.

For O1 here is what my research and testing would indicate- If you desire and edge quench, then O1 is going to work against you no matter what you try, that steel was designed to harden as completely and as evenly as possible, for that 52100 would be a little better. It is possible you could get some better results with limited equipment by multiple quenches over a single quench with a torch, if you are very careful and manage to avoid many hazards. However, with equipment that allows total control over the temperature and the ability to soak to manipulate those carbides, the differences will be striking. No matter what tools any of us use I think we can all agree that there is no substitute for control over the process and the more the better. On this I am so fanatical that I have invested much time and money in pursuit of it.

But above all, know what you want from your blades. If you wish to easily bend the blade there are techniques to achieve that. If you wish to cut certain materials with much more aggressiveness, there are treatments to use for that specialization. If you wish to cleave things some edge geometries will work better than if you simply want to slice a tomato. I could go on and on, but the confusion and misinterpretation of all those factors can be worse than no testing at all.
 
Kevin, thanks again for your expertise on 0-1. I just had a very nice reply typed in and by the time I was done,I was kicked off so I lost it all when I tried to submit [second time it's done that today!]. So now I'm mad and going to go play with my knives.The only thing worse than a dull knife is a computer!!!!!!!!!!!
 
On a seperate note,Kevin,that's a sweet piece over on the other pages. I'm always honored to accept info from such craftsmen.Someday I may know enough to improve another makers skills.
 
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