Heating above critical means you are forming a new set of austenite grains and then cooling to form pearlite. It is the rapid formation of new grains which helps to refine grain. If heating below transformation you are not forming new grains. You may be affecting the carbide structure which can have an indirect effect on the final heat treated grain size but it’s not the same thing.
I think I'm in need of an etchant. I've been advised by a chemist (I'm not the careless type, but I know there are plenty who are, so I understand the lack of availability and precautions) what the issues would be with nitric acid and methanol. that said, can you recommend any supply places in pittsburgh that would sell nital to someone off of the street? Doesn't need to be provided in a public response.
I've done a couple of samples of 1095 - these are hammered to shape by me then, ground, then heat treated in a simple small can forge, and then compared 1095 to a commercial file (they usually have nice fine grain that can be hard to match - I don't have a commercial 1095 sample to compare).
This is the file (as a starter for seeing relative grain size - the picture are optical around 50-75x (the hand scope makes fantastic claims, but the magnification is probably closer to the range I'm guessing)
This what 1095 looks like if it's heated above critical (but just barely) and cycled to black in air and then cycled to room temp on the third cycle and heated (never getting more than barely above nonmagnetic - no bright oranges or anything involved after shaping is done).
This is 1095 after the cycle of "not hotter than magnetic but close" heating mentioned above.
(by the way, I do have a proper budget metallurgical scope, but these irregular broken pieces are a no go as it's only good with dead flat surfaces vs. irregular broken-off bits)
both 1095 samples are untempered - they were cut from adjacent spots in the same piece of stock (after it was hammered to shape to become a chisel blank), just quenched in parks50, then transferred to icewater quickly and then put into the freezer. I don't have a hardness tester, but nothing above is close to being fileable.
The sample with the tiny grain is harder to break off in a vise. And separately, for confirmation, I have no furnace, so nothing is normalized - just heated to nonmagnetic, then "some more after that" and then quenched.
26c3 sees similar improvement, though there are little tiny black dots dispersed in the optical sample, which I'm assuming are carbon.
I have never done anything like this previously and have a metallurgical scope to grade sharpening stones by the edge they leave on a razor.
I *think* I'm inadvertently thermal cycling even though the steel samples are quenched in each cycle just before they would (by eye in dim light, and confirmed with a magnet) lose magnetism. The interim quenches are just done by a couple of dips in parks 50 (not fully to room temp).
I don't believe the file is a fair comparison to 1095 as I'm sure it has excess stuff in it, but it's my hurdle quenching in the shop at this point as in the past, I could break samples and tell by naked eye view that my attempts were far more coarse.
(I joined your patreon in exchange for being a nuisance)