Triple quench secrets to be revealed?(or not)

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Originally posted by Rick Baum
I haven’t had my blades tested for hardness or anything of that nature, so I only have my home test methods to compare it to. I definitely can’t say that my blades are fine grained but they do give me a good point of reference to try to improve upon in the future. I’m currently working on a blade right now that will be tested to destruction. I’ll let you know how that goes if you’d like.
Rick
Rick, many thanks. That gets the bulk of it in one thread... and I thank you for taking time to post, to type all this up. (wish my darned books weren't so terribly buried in dozens of moving box stacks).

I would like to know how the "tested to destruction" blade goes. I assume you are going to bend it in a vise back and forth until it snaps...?

You read my mind... I would humbly suggest you get a blade Rockwell tested (a local machine shop might do it pretty cheaply) just to see what Rc you are getting with that tempering protocol. Both blade and spine.

And now, of course, a few questions for my understanding. Selected snippets:
Originally posted by Rick Baum
I then anneal the blade three times.

Quenches - bring whole blade to non-magnetic (including the ricasso and quench approximately 1/3 of the blade in Texaco Quenchtex type A oil that is heated to 155-165 degrees. Place blade in home freezer until next quenching cycle. Repeat this process 2 more times for a total of 3 quench cycles.

1st temper - 2 hrs. at 330 degrees Place in the freezer...
2nd temper - 2 hrs. at 325 degrees. Placed in freezer ...
Cryo treatment in dry ice and kerosene for approximately 24 hrs. I figure it can’t hurt.
3rd temper - 2 hrs. at 315 degrees.

... test it for edge flexion using the “brass rod test”. I draw the full length of the blade’s edge on the brass rod 3 times on each side. (If it chips I re-temper at 20-25 degrees above my starting tempering heat of 330 degrees.)
Rick

During the heat/quench cycle, do you have a feel for how hot "non magnetic" is for your process? How long do you hold the blade at non-magnetic?

Have you ever tried a single quench?

Exactly how does one do a brass rod test? Brass rod in a vise? I assume you are bending knife's edge over? So you use two hands to hold the knife and bend knife edge, pulling across whole blade's edge? How far over are you bending the edge? 10 deg? 20 deg? 45 deg?

Any idea why the tempering temp drops by 5 degrees each time?

How often does edge chip and require that 4th temper?

Ever leave out the cryo to see if it is really doing anything for retained austenite, and does it improve toughness?

Said directly: an interesting approach to bladesmithing. It is however pretty labor intensive. Wonder which steps truly contribute to the grain refinement? Multiple normalizations? Low austenizing temp? Low soak times? Triple quench (and is this necessary based on low austenizing temps and short soak times?)
 
Rob,

Yes, it is very laborious to forge and HT a blade this way. But then... "Anything worth having is worth waiting for" right? Before I started to forge I made knives via stock removal for 4 years. All of them were made without the use of power tools except for a small drill press and a homemade buffer. I thought that by learning to forge I could cut down on some of the hrs. that it took me to make a knife especially the big ones. What was I thinking?:confused: But to be perfectly honest... If I could add a small fraction to the performance of my knives by doubling the amount of work that goes into them I would happily do it. I'm the type of person that is rarely satisfied. It is a personal motto of mine that "there is always one more thing that you can do". It's a real struggle some times for me having a motto like that but being inherently lazy. You should hear some of the arguments that I have with myself.:D
Anyway, I'm getting way off subject. To answer your questions:

Q - During the heat/quench cycle, do you have a feel for how hot "non magnetic" is for your process? How long do you hold the blade at non-magnetic?

A - I am definitely getting there but I will never give up the magnet, as far as I know it will never lie to me. I have never timed myself but I would guess I'm between 15-30 seconds at non-magnetic before the quench. It always takes about 15-20 minutes to get the blade evenly heated in my forge and as soon as it is evenly non-magnetic I put it back into the forge for about 10 seconds before it gets quenched.

Q - Have you ever tried a single quench?

A - Not yet. As soon as I get my ABS JS stamp out of the way I plan on doing a lot more experimenting. I really want to take a whole year to play around and see what works best for me before I start selling a lot of knives.

Q - Exactly how does one do a brass rod test? Brass rod in a vise? I assume you are bending knife's edge over? So you use two hands to hold the knife and bend knife edge, pulling across whole blade's edge? How far over are you bending the edge? 10 deg? 20 deg? 45 deg?

A - Yes, the brass or steel rod is firmly clamped horizontally in the jaws of the vise so that almost half of it's circumference is above the jaws. I then place the edge of the blade near the ricasso (at about the same angle that you would if you were sharpening it) onto the rod and try to press the edge into the rod, and then draw the blade back. The edge will deflect slightly at the point it makes contact with the rod. It takes some pretty good force to get it to deflect. I would guess that it deflects somewhere around 5 degrees??

Q - Any idea why the tempering temp drops by 5 degrees each time?

A - I wanted to make sure that I wasn't heating any higher than my first tempering temperature just to keep a handle on what was going on. This was an idea that I had a while before I started doing my own heat treating. Actually, I wanted to set my hardness with the first tempering cycle and then drop my temp by 10 degrees for the second and third tempering cycles. So if I tempered my blade at 330 degrees on the first cycle then the second and third would both ideally be at 320 degrees. My idea was confirmed when I recently read "Cryogenics" by William E. Bryson and he suggests a similar thing. If I remember correctly he suggested to drop each cycle by 10-15 degrees from the previous one.

Q - How often does edge chip and require that 4th temper?

A - I have been very fortunate and haven't had to re-temper any blades yet. I have a feeling that the one I'm working on now might be my first. I decided to temper it at 320 degrees on the first cycle. We'll see what happens.

Q - Ever leave out the cryo to see if it is really doing anything for retained austenite, and does it improve toughness?

A - Good question, I think you're reading my mind this time. The blade that I'm working on right now will not receive any cryo treatment prior to testing it for edge flex and cutting ability. When I have played with it for a while and am satisfied that I understand it's capabilities I'm going to cryo it in Liquid nitrogen and then temper it as close to the third tempering heat as I can. Without two nearly identical knives treated differently, hopefully this will give me some idea if there is a benefit to be had.

Mete, Thanks for your reply to my question a few pages ago. Actually, I got in a hurry when I asked the question and didn't word it properly. What I was wondering is this... When I edge quench a blade, the whole blade is at critical (non-magnetic) because I'm not using a torch to selectively heat the just the portion of the blade that will be quenched. Do you have any idea if the extra heat that is in the spine of the blade will have an effect on the martensite that is formed in the quenched part of the blade (help refine the grain in some way or produce a grain structure that consists of something other than just martensite and retained austenite?) I'm guessing, but I think it would take a lot longer to get all of the heat out of the blade during an edge quench than it would for a full quench. Is it possible that a triple edge quench would have a different grain structure (other than an obvious transition zone between the martensite and pearlite matrices) than a triple full quench (or single full quench for that matter)? All other variables being equal of course.
Thanks,
Rick
 
Rick, in edge quenching the quench should be a bit slower than in a full quench , but I don't know if it would be significant.A triple quench shouldn't change anything. I hope you or some other smith would do it my way.Single quench, single 400 temper and compare. These complicated HTs leave me shaking my head . I just read the articles on the Mad Dog Knives website again ,he uses O1 and differentially tempers the blade getting a large difference edge to spine .If I were a smith I would certainly try that.
 
.....Could you comment a little bit more about "hardened and tempered a lot" versus "never hardened"- spine problem. I think that smiths want also the spine be strong...

Possu, follow me. I'll try to put it all together. If you bought a hypo-eutectoid steel ( less than .85)such as 1050, It would consist of grains of pearlite and ferrite.By the time you get to a 1084 you would have all pearlite.Then you have something difficult to machine so you would generally get the steel in the spherodize anneal form where all the carbide is in the form of spheres, the matrix ferrite, much easier to machine. I would rather not have ferrite in the spine since while it's tough it's not strong. Lets leave it at that for now


By all means, as you wish, mete!


pig
 
Rick...

Now you did it...

When I read your posting where you said you..."used Load Control Shaft (high quality 5160) from the local John Deere dealership." i knew I had to go out to my John Deere dealership and ask around.

It was pouring down rain, and so I was muddy from work, so I drove around the back and found the shop guys were just watching the rain from the huge open door.

I asked to see what a used load shaft looked like, (I had never seen one in my whole life before...). after one guy passed me to another, we looked around and didnt find any old shafts...then the guy asked what I wanted it for, and when I told him that I had read that used load shafts make good knives, THEN the smiles came, and all the guys in the shop had to come running to see my own knife that I had on my belt. BOY did the guys there at that shop all want a knife made from a load shaft!...next thing I knew, all 10 guys are out digging in junk piles in the rain to dig out the only load shaft they had on hand...

GOT IT!...at last...

Now I have a question about what do do next with the shaft,,,,

All I got is a old style coal forge,,,and a hammer,,,and a small section of train Rail ....what do I do now?
 
Oh, man... then don't go to a chainsaw dealer ... or you'll have to learn how to make chainsaw damascus! Or a Harley dealer... Harley Chain damascus!

I have to admit though, that if I were a big Harley rider type, it WOULD be pretty cool to have a fixed or folder with a Harley chain damascus blade.
 
Rdangerer...

funny that you should say that....for my next door neighbor is a very good frind of mine, and he is a biker from the old days.....and,,,well, I wanted to learn that chain thingy in the future to make a knife from one of his old chains,,,,but thats another story,,,,,,
 
DaQo'tah,

If the shaft is one that has holes in both ends you will have to cut off one of the ends to get rid of the hole. I'm guessing that you will need to anneal the end of it before you could cut it with a hacksaw (if that's all you have). If there isn't a hole in one of the ends, just heat that end to your forging temp. and start hammering. Get ready for a bunch of hammering if you forge at the lower temps. like I do. I use a 3 lb. hammer and a section of railraod rail as well and it took me about 5 or 6 hrs. of heating and hammering to forge a 6" blade (7" including the ricasso). What is the diameter of the shaft that they found for you?

rdangerer, I'm not a farmer so I'll try to describe what a load control shaft is as best I can. When a tractor is pulling a plow or other implement there is a system built into the tractor that senses if the plow hits an immoveable object like a big rock. Somewhere on the tail end of the tractor is a round shaft made of 5160 spring steel (load control shaft) that is the connection between the plow and a hydrolic system that lifts plow in the event it hits something big, thus avoiding a lot of damage to the plow and or tractor. I'm sure there's a lot more to it than that but it should give you an idea. I'm told that these shafts are made of some of the most highly spec'ed 5160 available. John Deere go out of there way to make sure it meets their spec's.

Rick
 
DaQo'tah Forge,
there are advices and there are advices!!!!!!!!

I just worked with 1 inch by 1 inch tool steel piece, to build a helping tool.
Hard work with small coal forge and a hand powered sledge hammer, I have not a power hammer.I have 340 lbs anvil tough.

I think you have at practical level several not equally good options:

(1) Save money 2-3$/knife (what a proper dimensinoned steel is worth in a steel supply company / a big fixed blade) and buy a professional power hammer with some 7000$ (you can find an used good one even cheaper, but then you must use lot of time to find it and have to be lucky too). Well, I admit not to know exact American prices. I am quite sure that somebody will comment this like: I hear from my friend that his friend got a good power hammmer at 4990$, or something like that.

(2) Use your shaft (what ever it is, probably something big!), do not buy a power hammer and use first 100 years to split and forge to get nice pillets (with 3 lbs hammer :D:D:D-- :confused: ) , then start working with knifes. Because I do not know about the dimensions of "a saft", the time can be perhaps only 50 years or as well 200 years. Is 100 years waiting time too much? Are your customers impatient?
One "rule of thumb" of old smiths about heating in a small forge "inch and hour (depth)", even heating of big pieces takes time and then the real work starts.

(3) Buy some about 10$ priced nice dimensioned pieces of new 5160 or O-1 (few knifes from one piece) and work with knifes soon.

Pick your own choice with a great care, all pros and cons in mind! Mistake can be a serious one, if you choose a wrong option and stick with it.

One thing always in mind working with old used steel should be , the steel can have some very tiny internal damages not to be corrected by hammering at usual temperatures used in the blade work. What about your customers and possible damaged steel? Is it possible that "a saft" thrown away because of these damages appearing in a heavy work (even not easy to see)?
A steel can develop a stress as a human being, same reason often, too many times something.....

(I am very worried that I kill peter nap with laughing too much to compare humans and steels. Different things, I admit, literally speaking, which is the only way with......)

pig
 
RDangerer/Pig...

The Load control shaft is about 21 inches long and about 1 and 1/8 inch thick.

Thats dont seem to big for me to handle, after all, I was already hand forgeing on some truck springs that were over 1/2 inch easly. The only problem I face is that all the steel I have ever used so far has always been flat...The truck springs were curved, but still flat so this is going to be a new thing in my knife making . I never tried to turn a round thing into a flat thingy yet..

Oh, now when I went to the John Deere guys and asked to see a Load Control shaft, They all knew what one was right away...there was no question at all what I was seeking.

As at first they didnt think they had one on the scrap pile, they took me over to this HUGE tractor and showed me where they go...You cant actually see one when they are on the tractor,,,they run sideways between the rear wheels and seem to be connected to the hitch in some way I didnt understand.

The guys said that load control shafts wear out because of the way they are always under huge amounts of strain when you run the tractor and pull stuff.

I plan on forgeing two blades at first at the same time. one will be single Heat treated to check on some things I have been reading about, the other will be normal 3 HT.

You know,,I have been reading everyone's words and advice on this topic very carefully,,,and I have tried to understand as best I can what could be better Heat treatments for my blades...

and, to tell the truth, I like to do the 3 heat treatment quenches ...its fun to use my O/A torch, and by the time i finish the 3rd heat treatment quench, I have gotten good enough at it that the last one (the one that really counts) was done darn good!

However I hate to temper!...I hate to temper 3 times,,,,thats why I dont,,,I only temper once and then freeze the blade over night...I know this may or may not be a good idea,,,,But I hate to be stuck in the house waiteing for the oven timer to go "Ding!"
 
DaQo'tah Forge,
you should love tempering more, but you can't force the love!
Why you sould love tempering? The tempering many times is what everybody agrees Ed Fowler and metallurgists and ....

A good idea to try at least and see with "shaft" or something thick material.
My experience is that forging with hand hammer becomes surprisingly fast harder and harder when the thickness of the steel increases- when you find this yourself, believe your eyes, do not think that you are a poor smith and you just must learn to do it easily.

Good shafts: pig
 
rdangerer and DaQo'tah Forge are businessmen with their HD- chain knifes.

How to earn 1000000$ making knifes? Silly, at most possible to get minimum salary, a common idea.

There are a lot of 40-50 old HD- guys out there. Too much money in their pockets.

This idea probably would work. Marketing study. High prices. Brand. Nice design with something to do with HD. They buy at very high price (the higher the better), not for the better knife, but to show off to friends and to keep and strenghten their feelings and dreams. The business is mostly more selling dreams than enything else, the product comes as an additional minor factor. Who needs Atanta- olympic t- shirts as t- shirts. T- shirt is nothing important, the Atlanta olympics feeling and memory is.

But, why to make money, there are more important things, true?


pig
 
I found a piece of information in a book that says 5-10 min. soaktime for every 10 mm/~0,4" thickness( for low or not alloyed tool steels). I found this rule applied on this example:For a cold O2 blade and an oven at 800-810°C/~1472-1490°F hold 2-4 min. to heat up the blade (while opening keep the heat inside with a firebrick)and another 2-3 min. for soaktime ,depending of the thickness. I don´t know if it makes any difference, i just looked it up.

Thanks:)
 
Time for closing arguments?
Thanks to everybody. Talking is good, doing is even better?

My opinion:




blade.jpg


pig
 
yes nice tread
nice knife Pig and
I have to tell you Pig
though someone beat the he!L out of that anvil
of yours :D
 
Thanks Graymaker, I am not quilty to beat my dear tiny anvil to be said clearly and strongly, no space for suspicions.

Somebody did, yes, not among us any more for 100 years or so, went where we all are goining (, at least anvil beating people).

The anvil is Finnish Lokomo still in the production I guess.



pig
 
PIG....

The 1 and 1/8 inch John Deere Load Shaft was a bit of work....I started my forge at 8:00 on Sat morning,,,,and for a while, I didnt know if this was going to work for me,,,But I switched to my heavy hammer and really started to smack the steel as hard as I could,,,,,

I only use coal , and it was raining, But after one hour I rested about 1/2 way done,,,,,after lunch I finished within another hour and a half....

I spent the rest of the day working the blade, and its almost ready for the Heat treating....this blade will be Heat treated ONCE!.....

I have a 2nd blade in-work,,,

i will let you know,
 
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